ASTM D6349 Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry
ASTM D6349感應(yīng)耦合等離子體-原子發(fā)散光譜法測定由煤和焦炭燃燒產(chǎn)生的煤,焦炭和固體殘留物中主要和次要元素的標準試驗方法
A compositional analysis of coal and coke and their associated combustion residues are often useful in assessing their quality. Knowledge of the elemental composition of the associated residues is also useful in predicting the elemental enrichment/depletion compositional behavior of ashes and slags in comparison to the concentration levels in the parent coal. Utilization of the ash by-products and hazardous potential may also depend on the chemical composition and leachability of the inorganic constituents of the coal ash.
The chemical composition of laboratory-prepared ash may not exactly represent the composition of mineral matter in coal or the composition of fly ash and slag resulting from commerical-scale burning of the coal.
1. Scope
1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately)
ASTM Standards
D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D1193 Specification for Reagent Water
D2013 Practice for Preparing Coal Samples for Analysis
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D5142 Test Methods for Proximate Analysis of the Analysis Sample of Coal and Coke by Instrumental Procedures
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
D1193 Specification for Reagent Water
D2013 Practice for Preparing Coal Samples for Analysis
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D5142 Test Methods for Proximate Analysis of the Analysis Sample of Coal and Coke by Instrumental Procedures
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ISO Standard
ISO/IECGuide99:2007 International vocabulary of metrology -- Basic and general concepts and associated terms (VIM)
Index Terms
coal; coal ash; inductively coupled plasma-atomic emission spectrometry; major and minor element; Coal ash; Coal/coke products--chemical analysis; Composition analysis--coal/coke products; ICP-AES (inductively-coupled plasma atomic emission spectrometry); Major/minor elements;
